TA Instruments

AR1756-0009f

15/03/2013 15:08:49

Sample name	ASW Blank coupon#20 + DI + beads 275rad/s
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	9 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 15:08:49

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 275.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

1.0040	274.9	-731.66	10000	20.0	0.1909	1.004	-238.5	343.6	-0.6940	777.9	218.6520	6.587E-3	273.32	27332	3.411E-3	0.0	0.0
2.0200	275.0	562.94	10000	20.0	0.1771	2.020	183.5	343.7	0.5338	721.7	559.8370	6.108E-3	699.80	69980	3.411E-3	0.0	0.0
3.0040	275.0	579.19	10000	20.0	0.1792	3.004	188.8	343.7	0.5492	729.9	784.1140	6.178E-3	980.14	98014	3.411E-3	0.1	0.1
4.0040	275.0	575.08	10000	20.0	0.1806	4.004	187.4	343.7	0.5453	735.7	1011.6200	6.227E-3	1264.5	1.2645E5	3.411E-3	0.1	0.1
5.0040	275.0	576.60	10000	20.0	0.1721	5.004	187.9	343.8	0.5467	701.0	1349.6300	5.932E-3	1687.0	1.6870E5	3.411E-3	0.1	0.1
6.0200	275.0	562.86	10000	20.0	0.1767	6.020	183.5	343.8	0.5337	720.0	1578.2700	6.093E-3	1972.8	1.9728E5	3.411E-3	0.1	0.1
7.0200	275.0	563.85	10000	20.0	0.1761	7.020	183.8	343.7	0.5347	717.5	1916.4500	6.073E-3	2395.6	2.3956E5	3.411E-3	0.1	0.1
8.0040	275.0	554.95	10000	20.0	0.1771	8.004	180.9	343.8	0.5262	721.7	2141.3899	6.107E-3	2676.7	2.6767E5	3.411E-3	0.1	0.1
9.0200	275.0	558.85	10000	20.0	0.1777	9.020	182.2	343.7	0.5299	724.1	2483.3301	6.129E-3	3104.2	3.1042E5	3.411E-3	0.2	0.2
10.020	275.0	558.65	10000	20.0	0.1781	10.020	182.1	343.8	0.5297	725.8	2706.8101	6.142E-3	3383.5	3.3835E5	3.411E-3	0.2	0.2
11.020	275.0	543.73	10000	20.0	0.1789	11.020	177.2	343.8	0.5155	729.1	2935.9399	6.169E-3	3669.9	3.6699E5	3.411E-3	0.2	0.2
12.004	275.0	562.42	10000	20.0	0.1777	12.004	183.3	343.7	0.5334	724.1	3272.3501	6.130E-3	4090.4	4.0904E5	3.411E-3	0.2	0.2
13.096	275.0	559.49	10000	20.0	0.1757	13.096	182.4	343.8	0.5305	715.9	3499.9700	6.058E-3	4375.0	4.3750E5	3.411E-3	0.2	0.2
14.020	275.0	565.15	10000	20.0	0.1789	14.020	184.2	343.7	0.5359	729.1	3837.8000	6.170E-3	4797.3	4.7973E5	3.411E-3	0.2	0.2
15.020	275.0	552.26	10000	20.0	0.1751	15.020	180.0	343.8	0.5236	713.4	4063.8701	6.037E-3	5079.8	5.0798E5	3.411E-3	0.3	0.3
16.004	275.0	563.06	10000	20.0	0.1777	16.004	183.5	343.7	0.5339	724.1	4404.7900	6.129E-3	5506.0	5.5060E5	3.411E-3	0.3	0.3
17.020	275.0	560.69	10000	20.0	0.1714	17.020	182.8	343.7	0.5317	698.5	4629.5400	5.912E-3	5786.9	5.7869E5	3.411E-3	0.3	0.3
18.004	275.0	555.74	10000	20.0	0.1804	18.004	181.1	343.8	0.5269	734.9	4855.8599	6.219E-3	6069.8	6.0698E5	3.411E-3	0.3	0.3
19.020	275.0	573.97	10000	20.0	0.1745	19.020	187.1	343.8	0.5442	710.9	5194.8901	6.016E-3	6493.6	6.4936E5	3.411E-3	0.3	0.3
20.004	275.0	555.12	10000	20.0	0.1751	20.004	180.9	343.8	0.5263	713.4	5422.2402	6.036E-3	6777.8	6.7778E5	3.411E-3	0.3	0.3
21.004	275.0	560.51	10000	20.0	0.1769	21.004	182.7	343.7	0.5315	720.8	5760.3501	6.100E-3	7200.4	7.2004E5	3.411E-3	0.4	0.4
22.020	275.0	546.60	10000	20.0	0.1812	22.020	178.2	343.7	0.5183	738.2	5986.5801	6.248E-3	7483.2	7.4832E5	3.411E-3	0.4	0.4
23.024	275.0	562.36	10000	20.0	0.1822	23.024	183.3	343.8	0.5332	742.3	6334.3999	6.281E-3	7918.0	7.9180E5	3.411E-3	0.4	0.4
24.008	275.0	544.13	10000	20.0	0.1735	24.008	177.4	343.7	0.5160	706.8	6552.2202	5.982E-3	8190.3	8.1903E5	3.411E-3	0.4	0.4
25.004	275.0	548.45	10000	20.0	0.1779	25.004	178.8	343.8	0.5200	725.0	6779.5000	6.135E-3	8474.4	8.4744E5	3.411E-3	0.4	0.4
26.004	275.0	556.51	10000	20.0	0.1804	26.004	181.4	343.7	0.5277	734.9	7117.5400	6.220E-3	8896.9	8.8969E5	3.411E-3	0.4	0.4
27.024	275.0	548.30	10000	20.0	0.1804	27.024	178.7	343.7	0.5199	734.9	7345.5400	6.219E-3	9181.9	9.1819E5	3.411E-3	0.5	0.5
28.004	275.0	567.36	10000	20.0	0.1787	28.004	184.9	343.8	0.5380	728.3	7683.2598	6.163E-3	9604.1	9.6041E5	3.411E-3	0.5	0.5
29.004	275.0	557.03	10000	20.0	0.1783	29.004	181.6	343.7	0.5282	726.6	7909.2500	6.150E-3	9886.6	9.8866E5	3.411E-3	0.5	0.5
30.008	275.0	555.59	10000	20.0	0.1824	30.008	181.1	343.7	0.5268	743.2	8250.6904	6.289E-3	10313	1.0313E6	3.411E-3	0.5	0.5
31.020	275.0	565.64	10000	20.0	0.1696	31.020	184.4	343.7	0.5364	691.1	8475.9600	5.849E-3	10595	1.0595E6	3.411E-3	0.5	0.5
32.020	275.0	563.19	10000	20.0	0.1716	32.020	183.6	343.7	0.5340	699.3	8700.8896	5.919E-3	10876	1.0876E6	3.411E-3	0.5	0.5
33.024	275.0	532.67	10000	20.0	0.1808	33.024	173.6	343.8	0.5050	736.5	9040.3096	6.232E-3	11300	1.1300E6	3.411E-3	0.6	0.6
34.020	275.0	547.59	10000	20.0	0.1787	34.020	178.5	343.8	0.5192	728.3	9267.4805	6.163E-3	11584	1.1584E6	3.411E-3	0.6	0.6
35.000	275.0	553.85	10000	20.0	0.1755	35.000	180.5	343.8	0.5252	715.1	9605.7197	6.051E-3	12007	1.2007E6	3.411E-3	0.6	0.6
36.004	275.0	547.70	10000	20.0	0.1761	36.004	178.5	343.8	0.5193	717.5	9831.9902	6.072E-3	12290	1.2290E6	3.411E-3	0.6	0.6
37.004	275.0	556.15	10000	20.0	0.1755	37.004	181.3	343.7	0.5274	715.1	10171.600	6.052E-3	12715	1.2715E6	3.411E-3	0.6	0.6
38.020	275.0	554.49	10000	20.0	0.1779	38.020	180.7	343.8	0.5257	725.0	10397.500	6.134E-3	12997	1.2997E6	3.411E-3	0.6	0.6
39.020	275.0	563.71	10000	20.0	0.1769	39.020	183.7	343.7	0.5345	720.8	10623.500	6.101E-3	13279	1.3279E6	3.411E-3	0.7	0.7
40.020	275.0	546.80	10000	20.0	0.1767	40.020	178.2	343.8	0.5185	720.0	10967.600	6.093E-3	13710	1.3710E6	3.411E-3	0.7	0.7
41.004	275.0	566.48	10000	20.0	0.1749	41.004	184.6	343.8	0.5371	712.6	11190.800	6.030E-3	13989	1.3989E6	3.411E-3	0.7	0.7
42.004	275.0	559.37	10000	20.0	0.1710	42.004	182.3	343.7	0.5304	696.9	11530.100	5.898E-3	14413	1.4413E6	3.411E-3	0.7	0.7
43.008	275.0	562.35	10000	20.0	0.1702	43.008	183.3	343.8	0.5332	693.6	11758.700	5.868E-3	14698	1.4698E6	3.411E-3	0.7	0.7
44.008	275.0	557.38	10000	20.0	0.1731	44.008	181.7	343.8	0.5285	705.1	12094.900	5.966E-3	15119	1.5119E6	3.411E-3	0.7	0.7
45.020	275.0	554.21	10000	20.0	0.1747	45.020	180.6	343.7	0.5255	711.7	12320.200	6.024E-3	15400	1.5400E6	3.411E-3	0.8	0.8
46.004	275.0	569.34	10000	20.0	0.1775	46.004	185.6	343.7	0.5399	723.3	12546.200	6.122E-3	15683	1.5683E6	3.411E-3	0.8	0.8
47.004	275.0	548.79	10000	20.0	0.1794	47.004	178.9	343.8	0.5204	730.8	12885.700	6.184E-3	16107	1.6107E6	3.411E-3	0.8	0.8
48.020	275.0	553.56	10000	20.0	0.1743	48.020	180.4	343.8	0.5249	710.1	13114.100	6.009E-3	16393	1.6393E6	3.411E-3	0.8	0.8
49.004	275.0	549.37	10000	20.0	0.1822	49.004	179.1	343.8	0.5209	742.3	13451.100	6.282E-3	16814	1.6814E6	3.411E-3	0.8	0.8
50.004	275.0	562.61	10000	20.0	0.1812	50.004	183.4	343.7	0.5335	738.2	13677.400	6.248E-3	17097	1.7097E6	3.411E-3	0.8	0.8
51.004	275.0	556.74	10000	20.0	0.1698	51.004	181.5	343.8	0.5279	691.9	14018.300	5.855E-3	17523	1.7523E6	3.411E-3	0.9	0.9
52.004	275.0	561.11	10000	20.0	0.1723	52.004	182.9	343.7	0.5321	701.8	14243.500	5.940E-3	17804	1.7804E6	3.411E-3	0.9	0.9
53.004	275.0	570.45	10000	20.0	0.1718	53.004	185.9	343.7	0.5409	700.2	14469.000	5.926E-3	18086	1.8086E6	3.411E-3	0.9	0.9
54.020	275.0	539.25	10000	20.0	0.1800	54.020	175.8	343.7	0.5113	733.2	14809.700	6.206E-3	18512	1.8512E6	3.411E-3	0.9	0.9
55.020	275.0	562.25	10000	20.0	0.1733	55.020	183.3	343.7	0.5332	706.0	15035.600	5.976E-3	18795	1.8795E6	3.411E-3	0.9	0.9
56.004	275.0	547.84	10000	20.0	0.1761	56.004	178.6	343.7	0.5195	717.5	15373.600	6.073E-3	19217	1.9217E6	3.411E-3	0.9	0.9
57.020	275.0	556.76	10000	20.0	0.1706	57.020	181.5	343.7	0.5280	695.2	15601.800	5.884E-3	19502	1.9502E6	3.411E-3	1.0	1.0
58.004	275.0	571.36	10000	20.0	0.1710	58.004	186.2	343.7	0.5418	696.9	15939.200	5.898E-3	19924	1.9924E6	3.411E-3	1.0	1.0
59.004	275.0	554.05	10000	20.0	0.1767	59.004	180.6	343.7	0.5254	720.0	16165.400	6.094E-3	20207	2.0207E6	3.411E-3	1.0	1.0
60.004	275.0	569.81	10000	20.0	0.1757	60.004	185.7	343.7	0.5403	715.9	16391.600	6.058E-3	20490	2.0490E6	3.411E-3	1.0	1.0

